A one-dimensional Lanthanum sulphate [C4H16N3]2 [La2(SO4)6], I, has be prepared by interacting diethylenetriamine sulphate with La3+ ions at 100oC. The compound has been characterized with the help of powder x-ray analysis, scanning election microscopy, and infrared spectroscopy. The thermal behaviour of compound I has been studied by thermogravimetric analysis. Compound I crystallizes in monoclinic symmetry, space group P21/c (No. 14) with cell parameters a = 8.3305, b = 17.5000, c = 9.8407Å, ß = 101.610, vol = 143461Å. The inorganic framework [La2(SO4)6]6 - is anionic and charge compensation is achieved by incorporation of two molecules of fully-protonated diethylenetriamine.
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A. A. Ayi; I. E. Uwah; O. E. Offiong, "Linear chain Lanthanum Sulphate [C4H16N3]2 [La2(SO4) 6] obtained by reaction of La3+ ions with diethylenetriamine sulphate ", Journal of Ultra Chemistry, Volume 5, Issue 1, Page Number 13-20, 2018Copy the following to cite this URL:
A. A. Ayi; I. E. Uwah; O. E. Offiong, "Linear chain Lanthanum Sulphate [C4H16N3]2 [La2(SO4) 6] obtained by reaction of La3+ ions with diethylenetriamine sulphate ", Journal of Ultra Chemistry, Volume 5, Issue 1, Page Number 13-20, 2018Available from: http://www.journalofchemistry.org/paper/672/